Beamline Scientist Allen M. Orville
(631) 344-4739 amorv@bnl.gov

Spokesperson: Dieter Schneider (631) 344-3423 schneider@bnl.gov






   Beamline MicroSpectrophotometer Now Available
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Beamline MicroSpectrophotometer

The single crystal MicroSpectrophotometer system is mounted such that the optical focal point is coincident with the x-ray beam at x26c. This  enables correlated optical absorption spectroscopic data and diffraction data from the same crystal, without removing the sample from the diffractometer. A 25 micron region of the crystal is  probed and optical spectra are typically collected in approximately one second.  Redox active proteins and/or crystals containing optical chromophores are ideal candidates for this methodology.
Optical absortpion spectra can be collected between ~350-850 nm with samples held at 100K.

Crystals are mounted on a Crystal Logic diffractometer consisting of a mini-kappa goniometer (relocated from X25) and an ADSC Quantum 4 Detector.


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Benchtop MicroSpectrophotometer
Beamline Operation  and Beamline Characteristics
A single crystal MicroSpectrophotometer based upon the 4dx system is currently available. The Newport 75W Xe Research Arc Lamp OceanOptics USB4000 and SpectraSuite software package enable uv/vis absorption measurments between ~350-850 nm from ~25 micron region of the crystal. A coldstream will keep the sample at 100K.
X26C beamline safety checklist and BLOSA form
Beamline Merit Graphic Beamline.log
X26CPublications List
HKL2000site.def
Computers at X26C
Data Backup
Energy Range                      8-13 keV
Crystal Type                         Si(111)
Resolution (delta E/E)       1 x 10-3 to 1 x 10-4
Flux (photons/sec) at 1Å     0.5 x 10^11
and .2 mm aperture (300 mA, 2.6 GeV)
Spot Size -- focused 0.3H x 0.5V mm
Usual final aperture 0.2 mm
Total Horizontal Angular Acceptance 2 mradians
Flux curves for X26c

Last modified 19 May 2008 by AMO