| Beamline Scientist | Allen M. Orville |
(631) 344-4739 | amorv@bnl.gov | ||
| Spokesperson: | Dieter Schneider | (631) 344-3423 | schneider@bnl.gov | ||
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Beamline
MicroSpectrophotometer The single crystal
MicroSpectrophotometer system is mounted such
that the optical focal point is coincident with the x-ray beam at x26c.
This enables correlated optical absorption spectroscopic data and
diffraction data from the same
crystal, without removing the
sample from the diffractometer. A 25 micron region of the crystal
is probed and optical spectra are typically collected in
approximately one second. Redox active proteins and/or crystals
containing optical chromophores are ideal candidates for this
methodology.
Optical absortpion spectra can be collected between ~350-850 nm with samples held at 100K. Crystals are mounted on a Crystal Logic diffractometer consisting of a mini-kappa goniometer (relocated from X25) and an ADSC Quantum 4 Detector. |
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| Benchtop MicroSpectrophotometer | Beamline Operation and Beamline Characteristics | ||||
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X26C
beamline safety checklist and BLOSA
form Beamline Merit Graphic Beamline.log X26CPublications List HKL2000site.def Computers at X26C Data Backup Energy Range 8-13 keV Crystal Type Si(111) Resolution (delta E/E) 1 x 10-3 to 1 x 10-4 Flux (photons/sec) at 1Å 0.5 x 10^11 and .2 mm aperture (300 mA, 2.6 GeV) Spot Size -- focused 0.3H x 0.5V mm Usual final aperture 0.2 mm Total Horizontal Angular Acceptance 2 mradians |
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